Furfural diethyl acetal → HCID 15434861, 화합물

HRID 1604456

반응식

HRID 1604456 반응식
[CH2:1]([O:3][CH:4]([O:23][CH2:24][CH3:25])[C:5]1S[C:7]([Sn:10]([CH2:19][CH2:20][CH2:21][CH3:22])([CH2:15][CH2:16][CH2:17][CH3:18])[CH2:11][CH2:12][CH2:13][CH3:14])=[CH:8][CH:9]=1)[CH3:2].C([O:28]C(OCC)C1OC=CC=1)C>>[CH2:1]([O:3][CH:4]([O:23][CH2:24][CH3:25])[C:5]1[O:28][C:7]([Sn:10]([CH2:19][CH2:20][CH2:21][CH3:22])([CH2:15][CH2:16][CH2:17][CH3:18])[CH2:11][CH2:12][CH2:13][CH3:14])=[CH:8][CH:9]=1)[CH3:2]

참가 물질

3

반응물 2

HCID 83553Furfural diethyl acetalHCID 154348542-(Diethoxymethyl)-5-(tributylstannyl) thiophene

생성물 1

HCID 15434861HCID 15434861, 화합물수율 82%

실험 절차

Following the procedure for preparing 2-(diethoxymethyl)-5-(tributylstannyl)-thiophene as described in step (1) of Example 1, 17 g (10 mmol) of 2-(diethoxymethyl)furan was converted to 32.6 g (82% yield) of 2-(diethoxymethyl)-5-(tributylstannyl) furan (bp 110° C., 1 torr).

출처 및 근거

ORD 기록
ord-05e3189ee62643b59d248db4b713fd4b
출처 데이터셋
uspto-grants-1999_11
특허 번호
US05994394

연결된 노트

불러오는 중…