Boron tribromide → Phenol, 4-(2,2-difluorocyclopropyl)-

반응식

[F:1][C:2]1([F:13])[CH2:4][CH:3]1[C:5]1[CH:10]=[CH:9][C:8]([O:11]C)=[CH:7][CH:6]=1.B(Br)(Br)Br>>[F:1][C:2]1([F:13])[CH2:4][CH:3]1[C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1

참가 물질

반응물 2

HCID 25134Boron tribromide

HCID 21549152HCID 21549152, 화합물

생성물 1

HCID 21549151Phenol, 4-(2,2-difluorocyclopropyl)-

실험 절차

p-(2,2-Difluorocyclopropyl)phenol was prepared from 120 g. of p-(2,2-difluorocyclopropyl)anisole and 81 g. of boron tribromide according to the procedure described above in Example 1, part (c), affording 72 g. of oil used directly in the following reaction.

후처리

customaffording 72 g
customof oil used directly in the following reaction

출처 및 근거

ORD 기록: ord-9760bec5e0814e4fb5ceb31c1e14c843
출처 데이터셋: uspto-grants-1976_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03948973

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