Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloroform → 2-(4-Acetylphenoxy)-2-methylpropionic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloroform | HCID 6212 | — |
| 반응물 | 4'-Hydroxyacetophenone | HCID 7469 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 2-(4-Acetylphenoxy)-2-methylpropionic acid | HCID 104106 | — |
반응 단계
2-(p-Acetylphenoxy)-2-methylpropionic acid was prepared from 545 g. of p-hydroxyacetophenone, 960 g. of sodium hydroxide and 715 g. of chloroform in 11 liters of acetone according to the procedure described above in Example 1, part (d). The product was recrystallized from carbon tetrachloride and from isopropyl acetate to give 2-(p-acetylphenoxy)-2-methylpropionic acid as a pale cream solid, m.p. 108°-110°C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03948973 |
| 출처 데이터셋 | uspto-grants-1976_04 |
| ORD ID | ord-43972321ca904c3ca0b13546863795ca |
| 출처 메모 | uspto-grants-1976_04 |