참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Acetanilide | HCID 904 | — |
| 반응물 | 1,1-Dichloroethane | HCID 6365 | — |
| 반응물 | Benzoyl chloride | HCID 7412 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 생성물 | N-(4-benzoylphenyl)acetamide | HCID 228532 | — |
반응 단계
An ice-cooled solution of 5 grams of acetanilide and 15 g. of aluminum chloride in 75 ml. of dichloroethane is treated with 5 g. of benzoyl chloride in portions. The mixture is then heated at 80° C for 3 hours, decomposed with ice and dilute hydrochloric acid and the resulting solid isolated by suction filtration and recrystallized from ethanol:water to give p-benzoylacetanilide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US03949084 |
|---|
| 출처 데이터셋 | uspto-grants-1976_04 |
|---|
| ORD ID | ord-7671b3111bdd4df8ac7ebec234f49312 |
|---|
| 출처 메모 | uspto-grants-1976_04 |
|---|
