3-Amino-5-nitro-4-phenylbenzoic acid → HCID 21546851, 화합물

HRID 1605576노트

반응식

HRID 1605576 반응식
N[C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([N+]([O-])=O)[C:10]=1C1C=CC=CC=1)[C:5](O)=O.[NH2:20][C:21]1[CH:22]=[C:23]([CH:27]=[C:28]([S:36](=[O:39])(=[O:38])[NH2:37])[C:29]=1[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1)[C:24]([OH:26])=[O:25]>>[CH2:5]([NH:20][C:21]1[CH:22]=[C:23]([CH:27]=[C:28]([S:36](=[O:39])(=[O:38])[NH2:37])[C:29]=1[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1)[C:24]([OH:26])=[O:25])[C:4]1[CH:8]=[CH:9][CH:10]=[CH:2][CH:3]=1

참가 물질

3

반응물 2

HCID 124087693-Amino-5-nitro-4-phenylbenzoic acidHCID 215468413-Amino-4-phenyl-5-sulfamylbenzoic acid

생성물 1

HCID 21546851HCID 21546851, 화합물

실험 절차

By replacing in Example 1, step D, 3-amino-5-nitro-4-phenylbenzoic acid with an equimolar amount of 3-amino-4-phenyl-5-sulfamylbenzoic acid, and following the procedure described, 3-benzylamino-4-phenyl-5-sulfamylbenzoic acid is obtained with a melting point of 221°-222° C. The material is identical (IR, analysis) with the material prepared as in Example 1, step G.

출처 및 근거

ORD 기록
ord-43952021a45144c4b8cff70b9a11bdec
출처 데이터셋
uspto-grants-1976_04
특허 번호
US03950380

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