Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Peracetic Acid → 4-Tert-octylcatechol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Peracetic Acid | HCID 6585 | — |
| 반응물 | 4-Tert-octylphenol | HCID 8814 | — |
| 반응물 | Perpropionic acid | HCID 65136 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 4-Tert-octylcatechol | HCID 70828 | 61% |
반응 단계
The procedure of Example 8 was followed, except 20 ml of acetone was added as a solvent for para-tert.-octyl phenol and 4.5g (0.05 mol) of perpropionic acid in the form of about 25 weight% acetone solution was added over 20 minutes in place of peracetic acid. Consequently, the conversion of para-tert.-octyl phenol was 6.8%, 4-tert.-octyl pyrocatechol was formed in a yield of 61% based on the converted octyl phenol and the conversion of perpropionic acid was 100%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03950437 |
| 출처 데이터셋 | uspto-grants-1976_04 |
| ORD ID | ord-021a4408e9c9420987461663e7b55917 |
| 출처 메모 | uspto-grants-1976_04 |