2-Chlorobenzylhydrazine → HCID 20367316, 화합물

HRID 1605737노트

반응식

HRID 1605737 반응식
C([O:3][C:4](=O)[C:5](OCC)=[CH:6][NH2:7])C.[Cl:12][C:13]1[CH:21]=[CH:20][CH:19]=[CH:18][C:14]=1[CH2:15][NH:16][NH2:17]>>[NH2:7][C:6]1[NH:17][N:16]([CH2:15][C:14]2[CH:18]=[CH:19][CH:20]=[CH:21][C:13]=2[Cl:12])[C:4](=[O:3])[CH:5]=1

참가 물질

3

반응물 2

HCID 4170642-ChlorobenzylhydrazineHCID 86733242HCID 86733242, 화합물

생성물 1

HCID 20367316HCID 20367316, 화합물수율 40%

실험 절차

35 g of β-amino--ethoxyacrylic acid ethyl ester and 32 g of 2-chlorobenzylhydrazine when reacted as described in Example 45 yield 17.5 g of the compound identified above as colorless crystals of melting point 153°. (Yield: 40% of theory)

출처 및 근거

ORD 기록
ord-f1f2abed138c476b963969ea27f82ece
출처 데이터셋
uspto-grants-1976_04
특허 번호
US03950528

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