Hexadec-1-ene-1-sulfonic acid → 1-Hexadecene

HRID 1605806노트

반응식

HRID 1605806 반응식
[CH:1](S(O)(=O)=O)=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>CC(C)=O>[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

참가 물질

3

반응물 1

HCID 107566Hexadec-1-ene-1-sulfonic acid

생성물 1

HCID 123951-Hexadecene

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

The aqueous-acetone layer which contained the sulfonic acid fraction of the product was stripped of solvents at 40°-45°C. under a vacuum to give 2.85 g. of viscous acid identified as hexadecene sulfonic acid on the basis of an IR spectrum which showed the presence of trans olefinic double bond (965 cm-1) and the absence of sultones (no 830 and 530 cm-1 bands).

후처리

  1. customwas stripped of solvents at 40°-45°C. under a vacuum
  2. customto give 2.85 g

출처 및 근거

ORD 기록
ord-47b3cf032cd04a88af3fdbac6b14dce9
출처 데이터셋
uspto-grants-1976_04
특허 번호
US03951823

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