Cyclopropylamine → HCID 21545717, 화합물

HRID 1605997노트

반응식

HRID 1605997 반응식
Cl[C:2]1[C:3](=[O:14])[C:4]2[CH:5]=[N:6][N:7]([CH3:13])[C:8]=2[C:9](=[O:12])[C:10]=1[Cl:11].[CH:15]1([NH2:18])[CH2:17][CH2:16]1>C(O)C>[Cl:11][C:10]1[C:9](=[O:12])[C:8]2[N:7]([CH3:13])[N:6]=[CH:5][C:4]=2[C:3](=[O:14])[C:2]=1[NH:18][CH:15]1[CH2:17][CH2:16]1

참가 물질

4

반응물 2

HCID 69828CyclopropylamineHCID 12201360HCID 12201360, 화합물

생성물 1

HCID 21545717HCID 21545717, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

5,6-Dichloro-1-methyl-1H-indazole-4,7-dione (10 grams prepared as in Example I) and cyclopropylamine (10 grams) in ethanol (50 milliliters) were stirred together at room temperature for 30 minutes. The precipitate formed was filtered off and dried to yield the desired product as a red solid having a melting point of 175°-176° C.

후처리

  1. customThe precipitate formed
  2. filtrationwas filtered off
  3. customdried

출처 및 근거

ORD 기록
ord-34a39fc10d3a4f37aab710894e1623a0
출처 데이터셋
uspto-grants-1976_04
특허 번호
US03952003

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