참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Diethyl Sulfate | HCID 6163 | — |
| 반응물 | O-ethyl N,N-diisobutyl-thiocarbamate | HCID 21542997 | — |
| 생성물 | Butylate | HCID 16181 | 92% |
반응 단계
43.4 g. (0.2 mole) of O-ethyl N,N-diisobutyl-thiocarbamate are introduced into a 100 ml. round-bottomed flask, and 2.5 g. of diethyl sulfate are added. The mixture is refluxed for 90 minutes on an oil bath heated to 160°C, and thereafter the product is isolated by vacuum distillation. 39.8 g. (92 %) of S-ethyl N,N-diisobutyl-thiocarbamate are obtained; b.p.: 137°-138°C/20 Hgmm., nD25 = 1.4689.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US03953427 |
|---|
| 출처 데이터셋 | uspto-grants-1976_04 |
|---|
| ORD ID | ord-cd703b39e32d40d6a0aad0997c8a403a |
|---|
| 출처 메모 | uspto-grants-1976_04 |
|---|
