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Dichloromethane → 1175-97-9

HRID 1606423
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인쇄 미리보기

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HRID 1606423 반응식
Cl[CH2:2]Cl.[CH3:4][C:5]1([CH3:27])[S:9][C@@H:8]2[C@H:10]([NH:13][C:14]([C@H:16]([NH2:23])[C:17]3[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=3)=[O:15])[C:11](=[O:12])[N:7]2[C@H:6]1[C:24]([OH:26])=[O:25].O.O.O.S([O-])([O-])(=O)=O.[Mg+2]>C(N(CC)CC)C>[CH3:4][C:5]1([CH3:27])[S:9][C@@H:8]2[C@H:10]([NH:13][C:14]([C@H:16]([NH2:23])[C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[O:15])[C:11](=[O:12])[N:7]2[C@H:6]1[C:24]([OH:26])=[O:25].[CH2:11]([N:7]([CH2:6][CH3:24])[CH2:8][CH3:2])[CH3:10]
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참가 물질

5

반응물 3

HCID 6344DichloromethaneHCID 23565Ampicillin TrihydrateHCID 24083Sulfuric acid magnesium salt (1:1)

생성물 1

HCID 129189941175-97-9

시약·촉매·용매 1

HCID 8471Triethylamine용매

실험 절차

To 14 ml. of dichloromethane were added 806 mg. of ampicillin trihydrate, 600 mg. of magnesium sulfate, and 0.42 ml. of triethylamine and after stirring the mixture for about 1 hour at room temperature, magnesium sulfate was filtered off to provide a dichloromethane solution of ampicillin triethylamine salt.

후처리

  1. filtrationmagnesium sulfate was filtered off

출처 및 근거

ORD 기록
ord-0a4a0ff74e6f433db547a5ffd3334b16
출처 데이터셋
uspto-grants-1976_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US03953428

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