Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 4-Methylthio-3-(trifluoromethyl)phenylboronic acid pinacol ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Pinacol | HCID 6425 | — |
| 반응물 | 4-Methylthio-3-(trifluoromethyl)phenylboronic acid | HCID 74891169 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 4-Methylthio-3-(trifluoromethyl)phenylboronic acid pinacol ester | HCID 67277301 | — |
반응 단계
The product of step b) (0.25 g) was heated in dioxan (2 ml) with pinacol (2 equiv) for 3 h. The solution was treated with diethyl ether and water. The organic layer was separated, washed with brine, dried (Na2SO4) and concentrated in vacuo. Yield 85 mg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07737135B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-4377e4d71b804528910e589e09a43d88 |
| 출처 메모 | uspto-grants-2010_06 |