Acetaldehyde → Quindoxin

HRID 1607718

반응식

HRID 1607718 반응식
[CH:1]1[CH:9]=[CH:8][C:7]2[C:3](=[N:4][O:5][N+:6]=2[O-:10])[CH:2]=1.[CH:11](=O)[CH3:12]>C(N(CC)CC)C>[CH:9]1[CH:8]=[C:7]2[N:6]([O-:10])[CH:11]=[CH:12][N+:4](=[O:5])[C:3]2=[CH:2][CH:1]=1

참가 물질

4

반응물 2

HCID 177AcetaldehydeHCID 68075Benzofuroxan

생성물 1

HCID 72073Quindoxin

시약·촉매·용매 1

HCID 8471Triethylamine용매

실험 절차

A mixture of benzofuroxan (2.5 g.), acetaldehyde (2.5 ml.) and triethylamine (20 ml.) is allowed to stand at room temperature for 24 hours. The solid material which precipitates is filtered and dried to give product, M.P. 223°-224° C. dec. (MIC against P. vulgaris is 12.5 mcg./ml.).

후처리

  1. customThe solid material which precipitates
  2. filtrationis filtered
  3. customdried
  4. customto give product, M.P. 223°-224° C. dec. (MIC against P. vulgaris is 12.5 mcg./ml.)

출처 및 근거

ORD 기록
ord-8ce7d3dd4f95463ab3b62df2f02df71b
출처 데이터셋
uspto-grants-1989_09
특허 번호
US04866175

연결된 노트

불러오는 중…