Hydroquinone → 4-n-Butylbenzoic acid 4-(4'-methyldecyloxy)phenyl ester

HRID 1607774노트

반응식

HRID 1607774 반응식
CC(CCCCC)[CH2:3][CH2:4][CH2:5][CH2:6][C:7]1[CH:15]=[CH:14][C:10]([C:11]([OH:13])=[O:12])=[CH:9][CH:8]=1.[CH2:21](OC1C=CC(O)=CC=1)CCCCCCC.C(C1C=CC(C(O)=O)=CC=1)CCC.C[CH:51]([CH2:65][CH2:66][CH2:67][CH3:68])[CH2:52][CH2:53][CH2:54][CH2:55][CH2:56][O:57][C:58]1[CH:63]=[CH:62][C:61](O)=[CH:60][CH:59]=1.CC(CCCC)CCCCCBr.C1(C=CC(O)=CC=1)O>>[CH3:21][CH:53]([CH2:52][CH2:51][CH2:65][CH2:66][CH2:67][CH3:68])[CH2:54][CH2:55][CH2:56][O:57][C:58]1[CH:59]=[CH:60][C:61]([O:13][C:11](=[O:12])[C:10]2[CH:9]=[CH:8][C:7]([CH2:6][CH2:5][CH2:4][CH3:3])=[CH:15][CH:14]=2)=[CH:62][CH:63]=1

참가 물질

7

반응물 6

HCID 785HydroquinoneHCID 77412Phenol, 4-(octyloxy)-HCID 886314-Butylbenzoic acidHCID 144955834-(6'-Methyldecyloxy)-phenolHCID 14496338HCID 14496338, 화합물HCID 198510754-(5'-Methyldecyl)benzoic acid

생성물 1

HCID 543941834-n-Butylbenzoic acid 4-(4'-methyldecyloxy)phenyl ester

실험 절차

The procedure of Example 1 was followed except that the 4-(5'-methyldecyl)benzoic acid and 4-n-octoxyphenol were replaced by 4-n-butylbenzoic acid and 4-(6'-methyldecyloxy)-phenol prepared by reacting 6-methyldecylbromide with hydroquinone to thereby give the title compound.

후처리

  1. customprepared

출처 및 근거

ORD 기록
ord-1398138cb3c54dae89a6d1a7a98c392a
출처 데이터셋
uspto-grants-1989_09
특허 번호
US04866199

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