Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Butyric acid (4-quinolinylmethylene)hydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Butyrohydrazide | HCID 77079 | — |
| 반응물 | 4-Quinolinecarboxaldehyde | HCID 78072 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Butyric acid (4-quinolinylmethylene)hydrazide | HCID 86743403 | 85.4% |
반응 단계
A mixture of 7.85 gm (0.05 mole) of 4-quinolinecarboxaldehyde, 5.11 gm (0.05 mole) of butyric acid hydrazide and 100 ml of ethanol is refluxed 4 hr. The reaction mixture is diluted with water and cooled to room temperature. The mixture is chilled. The solid that separates is collected, washed with water and dried to give 10.3 gm of the title compound, having a melting point of 130.4° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04870082 |
| 출처 데이터셋 | uspto-grants-1989_09 |
| ORD ID | ord-86b41a2e023d46cfa519dc8f0d867f61 |
| 출처 메모 | uspto-grants-1989_09 |