Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl Alcohol → (3-Allyl-)heptafluorobutan-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl Alcohol | HCID 7858 | — |
| 반응물 | 1,1,1,2,3,4,4,4-Octafluorobut-2-ene | HCID 9678 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | (3-Allyl-)heptafluorobutan-2-one | HCID 22074693 | — |
반응 단계
396 g (1.98 mol) of octafluorobut-2-ene is condensed into 116 g (2 mol) of allyl alcohol at -5° C. Then 113 g (1.98 mol) of KOH, dissolved in 150 ml of water, is slowly added dropwise over the course of 3 hours, the temperature being maintained at 0°-5° C. Stirring continues overnight at room temperature and working-up is performed in the same way as in Example 2a.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05399645 |
| 출처 데이터셋 | uspto-grants-1995_03 |
| ORD ID | ord-5344c9fec59d4d58975ffa741fb2bfb6 |
| 출처 메모 | uspto-grants-1995_03 |