alpha-Hydroxyacetophenone → HCID 776385, 화합물

HRID 1609242노트

반응식

HRID 1609242 반응식
[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4](Cl)=[O:5].O[CH2:12][C:13]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:14]>>[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]1[O:5][C:16]2[CH:17]=[CH:18][CH:19]=[CH:20][C:15]=2[C:13](=[O:14])[CH:12]=1

참가 물질

3

반응물 2

HCID 68490alpha-HydroxyacetophenoneHCID 702762-Methylbenzoyl chloride

생성물 1

HCID 776385HCID 776385, 화합물

실험 절차

7 is prepared from 2-methylbenzoyl chloride (8) and 2-hydroxyacetophenone by the procedure of Example 1. The material is purified by vacuum column (eluting with 10% ethyl acetate in hexane), yielding 7 with a melting point of 45.5°-47.5° C.

후처리

  1. customThe material is purified by vacuum column (eluting with 10% ethyl acetate in hexane)
  2. customyielding 7 with a melting point of 45.5°-47.5° C.

출처 및 근거

ORD 기록
ord-9d226149205e428da9ef06116dc8a5e7
출처 데이터셋
uspto-grants-1995_03
특허 번호
US05399584

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