Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium → HCID 178444960, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium | HCID 5360545 | — |
| 반응물 | HCID 178444959 | HCID 178444959 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | HCID 178444960 | HCID 178444960 | 92.5% |
반응 단계
In 30 ml of ether was dissolved 2.0 g of N-[2-[3-[1-(1H-tetrazol-5-yl)ethoxy]phenoxy]phenyl]-4-hexyloxybenzamide followed by addition of a solution of 90 mg of sodium in ethanol, and the mixture was concentrated in vacuo to dryness. After addition of isopropyl ether, the resulting foamy solid was pulverized, filtered and dried to give 1.9 g of the sodium salt as a white amorphous powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05399703 |
| 출처 데이터셋 | uspto-grants-1995_03 |
| ORD ID | ord-d1a9acbae6d7492d8361972f84ec0462 |
| 출처 메모 | uspto-grants-1995_03 |