Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → ethyl-2-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Ethyl L-cysteinate | HCID 13359 | — |
| 반응물 | 2,4-Dimethoxybenzonitrile | HCID 77750 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | ethyl-2-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylate | HCID 17747724 | — |
반응 단계
2,4-Dimethoxybenzonitrile, (R)-cysteine ethyl ester and about 5 equivalents of triethylamine are refluxed in ethanol for about 6–8 hours to obtain ethyl-2-(2,4-dimethoxyphenyl)-4,5-dihydro-thiazole-4-(R)-carboxylate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06982335B2 |
| 출처 데이터셋 | uspto-grants-2006_01 |
| ORD ID | ord-495c069965fd4491b5366627893a9e8e |
| 출처 메모 | uspto-grants-2006_01 |