3,5-Dimethoxybenzyl Bromide → 1-(3,5-Dimethoxybenzyl)-5-isopropyl-6-(3,5-dimethyl-phenyl)thio-2,4-pyrimidinedione

HRID 1611307

반응식

HRID 1611307 반응식
[CH:1]([C:4]1[C:5](=[O:20])[NH:6][C:7](=[O:19])[NH:8][C:9]=1[S:10][C:11]1[CH:16]=[C:15]([CH3:17])[CH:14]=[C:13]([CH3:18])[CH:12]=1)([CH3:3])[CH3:2].[CH3:21][O:22][C:23]1[CH:24]=[C:25]([CH:28]=[C:29]([O:31][CH3:32])[CH:30]=1)[CH2:26]Br>>[CH3:32][O:31][C:29]1[CH:28]=[C:25]([CH:24]=[C:23]([O:22][CH3:21])[CH:30]=1)[CH2:26][N:8]1[C:9]([S:10][C:11]2[CH:12]=[C:13]([CH3:18])[CH:14]=[C:15]([CH3:17])[CH:16]=2)=[C:4]([CH:1]([CH3:3])[CH3:2])[C:5](=[O:20])[NH:6][C:7]1=[O:19]

참가 물질

3

반응물 2

HCID 12744903,5-Dimethoxybenzyl BromideHCID 104937275-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione

생성물 1

HCID 159577371-(3,5-Dimethoxybenzyl)-5-isopropyl-6-(3,5-dimethyl-phenyl)thio-2,4-pyrimidinedione수율 53.1%

실험 절차

5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione and 3,5-dimethoxybenzyl bromide were reacted by the same way with the example 1 to obtain the titled compound (234 mg, yield: 53.1%).

출처 및 근거

ORD 기록
ord-34fde574411242f68acc0bc3ba55c6a0
출처 데이터셋
uspto-grants-2006_01
특허 번호
US06987114B1

연결된 노트

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