Ammonia → HCID 10091730, 화합물
반응식
[O:1]1[C:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[OH:12])=[CH:4][CH:3]=[N:2]1.[OH:13][C:14]1[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=1)[C:17](OC)=O.[NH3:24]>>[O:1]1[C:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[O:12][CH2:8][CH2:7][CH2:6][CH:11]([CH3:10])[O:13][C:14]2[CH:23]=[CH:22][CH:21]=[C:16]3[C:15]=2[N:24]=[C:3]([NH2:2])[CH:4]=[CH:17]3)=[CH:4][CH:3]=[N:2]1참가 물질
4
실험 절차
The title compound was prepared according to the procedure described in Example 92 substituting 2-isoxazol-5-ylphenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, CDCl3) δ ppm 8.20 (d, 1H), 7.92 (d, 1H), 7.86 (dd, 1H), 7.34 (m, 1H), 7.23 (t, 1H), 7.16 (dd, 1H), 7.05 (d, 1H), 6.97 (m, 3H), 6.68 (d, 1H), 4.71 (m, 1H), 4.26 (m, 1H), 4.15 (m, 1H), 1.98–2.26 (m, 4H), 1.48 (d, 3H); MS (DCI/NH3) m/z 390 [M+H]+.
출처 및 근거
- ORD 기록
- ord-21e8e92c53ef4332af39bb08c7e8ccc3
- 출처 데이터셋
- uspto-grants-2006_01
- DOI