Potassium Carbonate → HCID 11289513, 화합물

HRID 1611974

반응식

HRID 1611974 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6](O)=[C:5]([O:10][CH3:11])[C:4]=1[O:12][CH3:13].C(=O)([O-])[O-:15].[K+].[K+].Br[CH2:21][CH2:22][CH2:23][C:24]([O:26][CH2:27][CH3:28])=[O:25]>CC(=O)CC>[CH3:11][O:10][C:5]1[CH:6]=[C:7]([CH:8]=[C:3]([O:2][CH3:1])[C:4]=1[O:12][CH3:13])[O:15][CH2:21][CH2:22][CH2:23][C:24]([O:26][CH2:27][CH3:28])=[O:25]

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 76300Ethyl 4-bromobutyrateHCID 6035772,3,4-Trimethoxyphenol

생성물 1

HCID 11289513HCID 11289513, 화합물

시약·촉매·용매 1

HCID 6569Methyl Ethyl Ketone용매

실험 절차

9.2 g of trimethoxyphenol, 14 g of potassium carbonate and 10.7 g of ethyl 4-bromobutanoate in 150 ml of 2-butanone are refluxed for 24 hours. The mineral salts are then filtered off and the solvent is distilled off under reduced pressure, enabling the expected compound to be obtained.

후처리

  1. filtrationThe mineral salts are then filtered off
  2. distillationthe solvent is distilled off under reduced pressure
  3. customto be obtained

출처 및 근거

ORD 기록
ord-029f660a4bf0481fa87428c8836f6e6b
출처 데이터셋
uspto-grants-2006_01
특허 번호
US06992085B2

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