Ethyl-1-indanone → 2-ethyl-2,3-dihydro-1H-inden-1-one oxime

HRID 1612261노트

반응식

HRID 1612261 반응식
O1C2C(=CC=CC=2)/C(=[N:11]/[OH:12])/CC1.[CH2:13]([CH:15]1[CH2:23][C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[C:16]1=O)[CH3:14]>>[CH2:13]([CH:15]1[CH2:23][C:22]2[C:17](=[CH:18][CH:19]=[CH:20][CH:21]=2)[C:16]1=[N:11][OH:12])[CH3:14]

참가 물질

3

반응물 2

HCID 5070076Ethyl-1-indanoneHCID 9673039Chroman-4-one oxime

생성물 1

HCID 738670832-ethyl-2,3-dihydro-1H-inden-1-one oxime

실험 절차

Following the procedure for the preparation of (4E)-2,3-dihydro-4H-chromen-4-one oxime but substituting (+/−)-2-ethyl-2,3-dihydro-1H-inden-1-one and making non-critical variations provided the title compound as a colorless syrup. MS (ESI+) for m/z 176.1 (M+H)+.

출처 및 근거

ORD 기록
ord-9400e1f8a5b540689adde0d6b5141f6d
출처 데이터셋
uspto-grants-2006_01
특허 번호
US06992087B2

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