Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Quinoline → (Z)-dodec-2-en-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Quinoline | HCID 7047 | — |
| 반응물 | Dodec-2-yn-1-ol | HCID 1712322 | — |
| 반응물 | 2-Decen-1-ol, (Z)- | HCID 5364953 | — |
| 생성물 | (Z)-dodec-2-en-1-ol | HCID 5364955 | — |
반응 단계
cis-2-Dodecen-1-ol was prepared as described above for cis-2-decen-1-ol except that 35 g of 2-dodecyn-1-ol, 1.0 g of catalyst, and 3.0 ml of quinoline was used. A clear oil, 33.86 g, was obtained after kugelrohr distillation. 1H NMR δ5.57 (m, 2), 4.19 (d, 2, J=5 Hz), 2.07 (dd, 2, J=6, 12 Hz), 1.5-1.2 (m, 14), 0.88 (t, 3, J=7 HZ).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05190969 |
| 출처 데이터셋 | uspto-grants-1993_03 |
| ORD ID | ord-29c445e10cd84eda8e1d41d37cdfb73e |
| 출처 메모 | uspto-grants-1993_03 |