Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Quinoline → cis-2-Tetradecen-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Quinoline | HCID 7047 | — |
| 반응물 | 2-Decen-1-ol, (Z)- | HCID 5364953 | — |
| 반응물 | 2-Tetradecynol | HCID 10965792 | — |
| 생성물 | cis-2-Tetradecen-1-ol | HCID 13313924 | — |
반응 단계
cis-2-Tetradecen-1-ol was prepared as described above for cis-2-decen-1-ol except that 1.0 g of 2-tetradecyn-1-ol, 50 mg of catalyst, and 0.10 ml of quinoline was used. A clear oil, 0.72 g, was obtained after kugelrohr distillation. 1H NMR δ5.57 (m, 2) 4.19 9d, 2, J=6 Hz), 2.07 (dd, 2, J=6, 13 Hz), 1.5-1.2 (m, 18), 0.88 (t, 3, J=7 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05190969 |
| 출처 데이터셋 | uspto-grants-1993_03 |
| ORD ID | ord-dffb8dfe60534d809cec0bef39e9f88e |
| 출처 메모 | uspto-grants-1993_03 |