참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nitrogen | HCID 947 | — |
| 반응물 | Stearic Acid | HCID 5281 | — |
| 반응물 | Pentaerythritol | HCID 8285 | — |
| 생성물 | Pentaerythrityl Tetrastearate | HCID 61037 | — |
반응 단계
A 1000 ml round bottomed flask was charged with 598.4 g. (0.12 mol) PEG 130 pentaerythritol and 36.3 g. (0.48 mol) triple pressed stearic acid. The mass was heated to 100° C. with a N2 sparge, 1.0 g. phosphoric acid and 0.1 g hypophosphorus acid were charged. The batch was heated to 215° C. while collecting the water of reaction, and maintained until an acid value of 11.5 was reached. The finished material was a grey waxy solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05192462 |
|---|
| 출처 데이터셋 | uspto-grants-1993_03 |
|---|
| ORD ID | ord-dfd81b29e6064084902fab84c97966fc |
|---|
| 출처 메모 | uspto-grants-1993_03 |
|---|
