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1-Diphenylmethoxy-2-(4-methoxyphenethylamino)-2-methylpropane → 1-Diphenylmethoxy-2-[N-(4-methoxyphenethyl)-N-methylamino]-2-methylpropane

HRID 1613176
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인쇄 미리보기

반응식

HRID 1613176 반응식
[C:1]1([CH:7]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[O:8][CH2:9][C:10]([NH:13][CH2:14][CH2:15][C:16]2[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=2)([CH3:12])[CH3:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:30]([BH3-])#N.[Na+].C=O>>[C:24]1([CH:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[O:8][CH2:9][C:10]([N:13]([CH2:14][CH2:15][C:16]2[CH:17]=[CH:18][C:19]([O:22][CH3:23])=[CH:20][CH:21]=2)[CH3:30])([CH3:11])[CH3:12])[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

3

반응물 2

HCID 197753321-Diphenylmethoxy-2-(4-methoxyphenethylamino)-2-methylpropaneHCID 131717802Sodium cyanoborohydride formaldehyde

생성물 1

HCID 197753191-Diphenylmethoxy-2-[N-(4-methoxyphenethyl)-N-methylamino]-2-methylpropane

실험 절차

The title compound was prepared as described in Example 5, Method A, using 1-diphenylmethoxy-2-(4-methoxyphenethylamino)-2-methylpropane (see Example 2) and sodium cyanoborohydride/formaldehyde. The title compound was obtained as a colourless oil (200 mg, 69%).

후처리

  1. customThe title compound was prepared

출처 및 근거

ORD 기록
ord-b1f801d918734ef8bec278fec03ee43d
출처 데이터셋
uspto-grants-1993_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05192765

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