Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Borane → 2-(3,4-Dichlorophenoxy)ethan-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Borane | HCID 6331 | — |
| 반응물 | (3,4-Dichlorophenoxy)acetic acid | HCID 11495 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-(3,4-Dichlorophenoxy)ethan-1-ol | HCID 19108692 | 91% |
반응 단계
The title compound was prepared by reduction of 2-(3,4-dichlorophenoxy)acetic acid (Aldrich, 96% pure) with borane in tetrahydrofuran (Aldrich, 1M solution) using the procedure of N. M. Yoon, et al. in J. Org. Chem 38(#16) p. 2786 (1973). The yield was 91% of theory.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05192785 |
| 출처 데이터셋 | uspto-grants-1993_03 |
| ORD ID | ord-7b0e61847cba4038b8a679e3b6d599da |
| 출처 메모 | uspto-grants-1993_03 |