Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyloctadecylamine → N-(2-(Benzoyloxy)ethyl)-N,N-dimethyl-n-octadecylammonium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyloctadecylamine | HCID 15365 | — |
| 반응물 | 2-Bromoethyl Benzoate | HCID 523090 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-(2-(Benzoyloxy)ethyl)-N,N-dimethyl-n-octadecylammonium bromide | HCID 19774320 | — |
반응 단계
A mixture of 45.0 g (0.1964 mol) of 2-bromoethyl benzoate and an equimolar amount of N,N-dimethyl-n-octadecylamine in 207 ml of acetonitrile was heated at reflux for 4.5 hours. The reaction mixture was then cooled. The solid was then collected, washed with ether, and dried to yield 76.7 g of the title compound; mp=87°-93° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05194472 |
| 출처 데이터셋 | uspto-grants-1993_03 |
| ORD ID | ord-5d30a4eeed0a41b5be19d5faad877ab9 |
| 출처 메모 | uspto-grants-1993_03 |