Chlorosulfamic acid → HCID 19108682, 화합물

반응식

[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][O:7][C:8]1[CH:17]=[CH:16][C:11]([O:12][CH2:13][CH2:14][OH:15])=[CH:10][CH:9]=1>>[S:1]([O:15][CH2:14][CH2:13][O:12][C:11]1[CH:16]=[CH:17][C:8]([O:7][CH3:6])=[CH:9][CH:10]=1)(=[O:4])(=[O:3])[NH2:2]

참가 물질

반응물 2

HCID 24499Chlorosulfamic acid

HCID 2200792-(4-Methoxyphenoxy)ethanol

생성물 1

HCID 19108682HCID 19108682, 화합물수율 54%

실험 절차

The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-(4-methoxyphenoxy)ethanol in 54% yield as an off-white solid, mp 84°-87° C.

출처 및 근거

ORD 기록: ord-cacb9ad89cfd4090a7e13ade92dea77f
출처 데이터셋: uspto-grants-1993_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05194446

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