Diethyl Ether → 3-Hydroxypropyl Dimethyl Nonyl Ammonium Iodide

HRID 1614032노트

반응식

HRID 1614032 반응식
[CH2:1]([I:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[CH3:11][N:12]([CH:14](O)[CH2:15][CH3:16])[CH3:13].CC[O:20]CC>C(#N)C>[I-:10].[OH:20][CH2:16][CH2:15][CH2:14][N+:12]([CH3:13])([CH3:11])[CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]

참가 물질

5

반응물 3

HCID 3283Diethyl EtherHCID 202751-IodononaneHCID 116739Propanol, (dimethylamino)-

생성물 1

HCID 197748283-Hydroxypropyl Dimethyl Nonyl Ammonium Iodide수율 77%

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

Employing the procedure of EXAMPLE II, 20.0 g of nonyl iodide was reacted with 14.3 ml of N,N-dimethylaminopropanol in 50 ml of acetonitrile to provide a crude product which was slurried with ether to give 27 g (77%) of an amber oil which solidified on standing. Proton NMR confirmed the desired structure.

후처리

  1. customto provide a crude product which

출처 및 근거

ORD 기록
ord-d2060ecb37a04a32893fe286ab4cde1e
출처 데이터셋
uspto-grants-1993_03
특허 번호
US05194667

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