2-Acrylamido-2-methyl-1-propanesulfonic acid → Ammonium acryloyldimethyltaurate

HRID 1614837

반응식

HRID 1614837 반응식
COCCOCC[N:8](CCOCCOC)CCOCCOC.[C:23]([NH:27][C:28]([CH3:35])([CH3:34])[CH2:29][S:30]([OH:33])(=[O:32])=[O:31])(=[O:26])[CH:24]=[CH2:25]>>[NH4+:8].[C:23]([NH:27][C:28]([CH3:35])([CH3:34])[CH2:29][S:30]([O-:33])(=[O:31])=[O:32])(=[O:26])[CH:24]=[CH2:25]

참가 물질

3

반응물 2

HCID 653602-Acrylamido-2-methyl-1-propanesulfonic acidHCID 112414Ethanamine, 2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]-

생성물 1

HCID 6850854Ammonium acryloyldimethyltaurate수율 99%

실험 절차

A nitrogen purged 50 ml schlenk flask was charged with freshly distilled tris[2-(2-methoxyethoxy)-ethyl]amine (1.69 g, 5.24 mmol) and 2-acrylamido-2-methyl-1-propanesulfonic acid (AMPS) (1.09 g, 5.24 mmol) and stirred at ambient temperature for 8 hr or until completely dissolved. Total dissolution completes formation of the AMPS-ammonium salt monomer as a transparent light amber oil in a 99% yield which was used immediately without further purification.

후처리

  1. customA nitrogen purged 50 ml schlenk flask
  2. dissolutionuntil completely dissolved
  3. dissolutionTotal dissolution
  4. customwas used immediately without further purification

출처 및 근거

ORD 기록
ord-d7f97ed05a4c4b279cb92f906eed8229
출처 데이터셋
uspto-grants-2014_07
특허 번호
USRE044988E1

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