Allyl bromide → HCID 10703113, 화합물

반응식

[O:1]1[C:5]2([CH2:10][CH2:9][CH2:8][C:7](=[O:11])[CH2:6]2)[O:4][CH2:3][CH2:2]1.[CH2:12](Br)[CH:13]=[CH2:14]>>[CH2:14]([C:7]1([OH:11])[CH2:8][CH2:9][CH2:10][C:5]2([O:4][CH2:3][CH2:2][O:1]2)[CH2:6]1)[CH:13]=[CH2:12]

참가 물질

반응물 2

HCID 7841Allyl bromide

HCID 2406021,4-Dioxaspiro[4.5]decan-7-one

생성물 1

HCID 10703113HCID 10703113, 화합물수율 84%

실험 절차

The title compound is prepared from 1,4-dioxa-spiro[4.5]decan-7-one and allyl bromide following a procedure analogous to that described in Step 1 of Intermediate 2. Yield: 84% of theory; Mass spectrum (ESI+): m/z=181 [M+H—H2O]+.

출처 및 근거

ORD 기록: ord-e61daed4c9604d74bbc7dcf51a112b28
출처 데이터셋: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08765744B2

반응 노트

불러오는 중…