Methanamine, N-methoxy-, hydrochloride (1:1) → HCID 86660998, 화합물

반응식

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([C:13]2[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][C:14]=2[CH3:20])[CH2:9][C:10](O)=[O:11])=[CH:4][CH:3]=1.Cl.[CH3:22][NH:23][O:24][CH3:25]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([C:13]2[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][C:14]=2[CH3:20])[CH2:9][C:10]([N:23]([O:24][CH3:25])[CH3:22])=[O:11])=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 81138Methanamine, N-methoxy-, hydrochloride (1:1)

HCID 66666388HCID 66666388, 화합물

생성물 1

HCID 86660998HCID 86660998, 화합물

실험 절차

In analogy to example 74, step 4, from 3-(4-bromophenyl)-3-(4-chloro-2-methylphenyl)-propanoic acid and N,O-dimethylhydroxylamine hydrochloride was prepared the title compound as a colorless oil, MS (ESI+): m/z=398.03 [M+H]+.

출처 및 근거

ORD 기록: ord-40dd9d154d6e400ab023f407bbb5b013
출처 데이터셋: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08765730B2

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