Acetic Acid → Tetraethylammonium acetate

반응식

[OH-].[CH2:2]([N+:4]([CH2:9][CH3:10])([CH2:7][CH3:8])[CH2:5][CH3:6])[CH3:3].[C:11]([OH:14])(=[O:13])[CH3:12]>>[C:11]([O-:14])(=[O:13])[CH3:12].[CH2:2]([N+:4]([CH2:9][CH3:10])([CH2:7][CH3:8])[CH2:5][CH3:6])[CH3:3]

참가 물질

반응물 2

HCID 176Acetic Acid

HCID 6509Tetraethylammonium Hydroxide

생성물 1

HCID 102017Tetraethylammonium acetate

실험 절차

An aqueous tetraethylammonium hydroxide solution (1 mol) was charged into a flask and, while the solution was cooled so as to maintain it at room temperature, acetic acid (1 mol) was added thereto to obtain a tetraethylammonium acetate salt. Thereafter, ethylene glycol was added as a solvent so as to be a predetermined concentration and then water was removed by evaporation using an evaporator to obtain a solution of 50% of tetraethylammonium acetate and 50% of ethylene glycol.

후처리

temperaturewas cooled so as

출처 및 근거

ORD 기록: ord-e53f35db58dc46019cb349d708d7aabe
출처 데이터셋: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08779018B2

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