Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1625192생성일: 2026년 10월 26일
O-(4-Nitrophenyl)hydroxylamine → (2-Butyl-5-nitrobenzofuran-3-yl)(4-methoxyphenyl)methanone
https://huagongshe.com/reaction/1625192
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | O-(4-Nitrophenyl)hydroxylamine | HCID 15562106 | — |
| 반응물 | 1-(4-Methoxyphenyl)-heptane-1,3-dione | HCID 44541818 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | (2-Butyl-5-nitrobenzofuran-3-yl)(4-methoxyphenyl)methanone | HCID 22595055 | 70% |
반응 단계
O-4-nitrophenylhydroxylamine (100 mg), was suspended in 0.5 ml acetic acid and 1-(4-methoxyphenyl)-heptane-1,3-dione was added. The mixture was stirred at 70° C. for 3 h and then at 100° C. for an additional 14 h. The mixture was cooled to room temperature and the solvent evaporated under vacuum. Yield 70% of 2-butyl-3-(4-methoxybenzoyl)-5-nitrobenzofuran.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08779201B2 |
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| 출처 데이터셋 | uspto-grants-2014_07 |
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| ORD ID | ord-3c7a7e1806bd48a19f946c7756e4e421 |
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| 출처 메모 | uspto-grants-2014_07 |
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