Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine → 2,4-Dimethylbenzohydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine | HCID 9321 | — |
| 반응물 | Methyl 2,4-dimethylbenzoate | HCID 32031 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2,4-Dimethylbenzohydrazide | HCID 4846173 | — |
반응 단계
To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08784782B2 |
| 출처 데이터셋 | uspto-grants-2014_07 |
| ORD ID | ord-0c7a3d9d10ba4e2b964212cfbbb97f70 |
| 출처 메모 | uspto-grants-2014_07 |