2-Phenylthiophene → 5-Bromo-2,4-dimethyl-1-(5-phenyl-2-thienylmethyl)benzene

HRID 1625872

반응식

[Br:1][C:2]1[C:3]([CH3:12])=[CH:4][C:5]([CH3:11])=[C:6]([CH:10]=1)[C:7](O)=O.[C:13]1([C:19]2[S:20][CH:21]=[CH:22][CH:23]=2)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[Br:1][C:2]1[C:3]([CH3:12])=[CH:4][C:5]([CH3:11])=[C:6]([CH2:7][C:21]2[S:20][C:19]([C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=3)=[CH:23][CH:22]=2)[CH:10]=1

참가 물질

반응물 2

HCID 699992-Phenylthiophene

HCID 5557655-Bromo-2,4-dimethylbenzoic acid

생성물 1

HCID 666089545-Bromo-2,4-dimethyl-1-(5-phenyl-2-thienylmethyl)benzene

실험 절차

The above 5-bromo-2,4-dimethylbenzoic acid and 2-phenylthiophene were treated in a manner similar to Reference Example 5 to give 5-bromo-2,4-dimethyl-1-(5-phenyl-2-thienylmethyl)benzene as colorless crystals. APCI-Mass m/Z 357/359 (M+H).

출처 및 근거

ORD 기록: ord-6888c55c752c4dd597dfcd6999041e8d
출처 데이터셋: uspto-grants-2014_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08785403B2

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