5-Bromo-2-chlorobenzaldehyde → HCID 66608064, 화합물

HRID 1625905노트

반응식

HRID 1625905 반응식
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[N:6]1[CH:10]=[CH:9][CH:8]=[N:7]1.[Br:11][C:12]1[CH:13]=[CH:14][C:15]([Cl:20])=[C:16]([CH:19]=1)[CH:17]=O>>[Br:11][C:12]1[CH:13]=[CH:14][C:15]([Cl:20])=[C:16]([CH2:17][C:5]2[S:1][C:2]([N:6]3[CH:10]=[CH:9][CH:8]=[N:7]3)=[CH:3][CH:4]=2)[CH:19]=1

참가 물질

3

반응물 2

HCID 106089255-Bromo-2-chlorobenzaldehydeHCID 125544841-(Thiophen-2-yl)-1H-pyrazole

생성물 1

HCID 66608064HCID 66608064, 화합물

실험 절차

1-(2-thienyl)pyrazole (see: Chemica Scripta (1979) 13, 157-161) and 5-bromo-2-chlorobenzaldehyde obtained in Reference Example 16-(1) were used and treated in a manner similar to Reference Example 7 to give the title compound as colorless solid. APCI-Mass m/z 353/355 (M+H).

후처리

  1. additiontreated in a manner similar to Reference Example 7

출처 및 근거

ORD 기록
ord-a9a11f3cf7d341fcb2651e810d3e254f
출처 데이터셋
uspto-grants-2014_07
특허 번호
US08785403B2

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