HCID 67496690, 화합물 → HCID 69620893, 화합물

HRID 1628295노트

반응식

HRID 1628295 반응식
[CH3:1][C:2]1[CH:7]=[C:6]([C:8]2[CH:9]=[C:10]([NH2:15])[CH:11]=[C:12]([NH2:14])[CH:13]=2)[CH:5]=[CH:4][N:3]=1.[O:16]=[C:17](NC1N=C(C2C=CN=CC=2)SC=1)[C@@H:18]([NH:26][C:27](=[O:33])[O:28][C:29]([CH3:32])([CH3:31])[CH3:30])[CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[NH2:14][C:12]1[CH:11]=[C:10]([NH:15][C:17](=[O:16])[C@@H:18]([NH:26][C:27](=[O:33])[O:28][C:29]([CH3:30])([CH3:31])[CH3:32])[CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:9]=[C:8]([C:6]2[CH:5]=[CH:4][N:3]=[C:2]([CH3:1])[CH:7]=2)[CH:13]=1

참가 물질

3

반응물 2

HCID 67496690HCID 67496690, 화합물HCID 69620697HCID 69620697, 화합물

생성물 1

HCID 69620893HCID 69620893, 화합물

실험 절차

This title compound was prepared from 51.1C (2.10 g, 10.0 mmol) according the procedure described above for conversion of 4.A to 4.B. The product 51.1D was purified by flash chromatography on silica gel using 0-7% MeOH/CH2Cl2 for elution.

후처리

  1. customThe product 51.1D was purified by flash chromatography on silica gel using 0-7% MeOH/CH2Cl2 for elution

출처 및 근거

ORD 기록
ord-8000ae479a6e40e5a413901779709bcc
출처 데이터셋
uspto-grants-2014_07
특허 번호
US08785468B2

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