Ethyl 3-(2-benzyloxy-ethoxy)-propionate → Ethyl 3-(2-hydroxyethoxy)propanoate
반응식
C([O:8][CH2:9][CH2:10][O:11][CH2:12][CH2:13][C:14]([O:16][CH2:17][CH3:18])=[O:15])C1C=CC=CC=1>C(O)C.[Pd]>[OH:8][CH2:9][CH2:10][O:11][CH2:12][CH2:13][C:14]([O:16][CH2:17][CH3:18])=[O:15]참가 물질
4
실험 절차
3.73 g (14.8 mmol) ethyl 3-(2-benzyloxy-ethoxy)-propionate are hydrogenated together with 665 mg 10% palladium charcoal in 70 ml of ethanol for 44 minutes at ambient temperature under a hydrogen atmosphere at 3 bar. Then the mixture is suction filtered and the filtrate is evaporated down i. vac.
후처리
- filtrationfiltered
- customthe filtrate is evaporated down i
출처 및 근거
- ORD 기록
- ord-b290823003c54c97b3e6ce44645532ec
- 출처 데이터셋
- uspto-grants-2014_07
- 특허 번호
- US08791103B2
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