Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Lithium Hydroxide → 3-(2-Chloroethoxy)propanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Lithium Hydroxide | HCID 3939 | — |
| 반응물 | Ethyl 3-(2-chloro-ethoxy)-propionate | HCID 85848654 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-(2-Chloroethoxy)propanoic acid | HCID 343680 | — |
반응 단계
2.00 g (11.1 mmol) ethyl 3-(2-chloro-ethoxy)-propionate are suspended in 8 ml of ethanol and 4.96 ml (16.6 mmol) of 8% lithium hydroxide solution are added. The mixture is stirred for 4 hours at ambient temperature, then evaporated down i. vac., acidified with 2-molar hydrochloric acid, combined with diethyl ether and dried over sodium sulphate. Then it is filtered off and evaporated down i. vac.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08791103B2 |
| 출처 데이터셋 | uspto-grants-2014_07 |
| ORD ID | ord-91e653f6c9934104be09a854ffda7f38 |
| 출처 메모 | uspto-grants-2014_07 |