3,5-Difluorobenzoic acid → 1-Methyl-4-nitrosopiperidin-4-yl 3,5-difluorobenzoate

HRID 1630431

반응식

HRID 1630431 반응식
[CH3:1][N:2]1[CH2:7][CH2:6][C:5](=[N:8][OH:9])[CH2:4][CH2:3]1.C([O-])(=O)C.C([O-])(=O)C.C([O-])(=O)C.C([O-])(=O)C.[Pb+4].[F:27][C:28]1[CH:29]=[C:30]([CH:34]=[C:35]([F:37])[CH:36]=1)[C:31]([OH:33])=[O:32]>>[F:27][C:28]1[CH:29]=[C:30]([CH:34]=[C:35]([F:37])[CH:36]=1)[C:31]([O:33][C:5]1([N:8]=[O:9])[CH2:6][CH2:7][N:2]([CH3:1])[CH2:3][CH2:4]1)=[O:32]

참가 물질

4

반응물 3

HCID 1012653,5-Difluorobenzoic acidHCID 3390531-Methylpiperidin-4-one oximeHCID 178418268HCID 178418268, 화합물

생성물 1

HCID 444796551-Methyl-4-nitrosopiperidin-4-yl 3,5-difluorobenzoate

실험 절차

1-Methyl-4-nitrosopiperidin-4-yl 3,5-difluorobenzoate is prepared from 1-methyl-piperidin-4-one oxime, lead tetraacetate and 3,5-difluorobenzoic acid using conditions of General Method 3.

출처 및 근거

ORD 기록
ord-d4309eb5fd934888b97699772b653dc3
출처 데이터셋
uspto-grants-2014_07
특허 번호
US08791134B2

연결된 노트

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