Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Methylpiperidin-4-one oxime → Dibutyl 1-methyl-4-nitrosopiperidin-4-yl phosphate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Methylpiperidin-4-one oxime | HCID 339053 | — |
| 반응물 | Dibutyl phosphate anion | HCID 3790919 | — |
| 반응물 | HCID 178418268 | HCID 178418268 | — |
| 생성물 | Dibutyl 1-methyl-4-nitrosopiperidin-4-yl phosphate | HCID 57954472 | — |
반응 단계
Dibutyl 1-methyl-4-nitrosopiperidin-4-yl phosphate was prepared from 1-methyl-piperidin-4-one oxime, lead tetraacetate and dibutyl phosphate using conditions of General Method 3. 1H NMR (360 MHz, chloroform-d) δ 4.03-4.17 (4H, m), 2.77-2.88 (2H, m), 2.27-2.40 (6H, m), 2.12-2.24 (4H, m), 1.59-1.83 (6H, m), 1.38 (4H, q, 7.2 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08791134B2 |
| 출처 데이터셋 | uspto-grants-2014_07 |
| ORD ID | ord-d66f9610286443bd9b81dc06709a5987 |
| 출처 메모 | uspto-grants-2014_07 |