Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aniline → N-(3-Methoxybenzylidene)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | 3-Methoxybenzaldehyde | HCID 11569 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | N-(3-Methoxybenzylidene)aniline | HCID 555084 | — |
반응 단계
A solution of 85.4 gm. of 3-methoxybenzaldehyde, 58.7 gm. of aniline, and 185 gm. of 3A molecular sieves in 700 ml. of anhydrous ether was refluxed for 16 hours. The ether was dried (Na2SO4), filtered, and concentrated in vacuo to an oil which upon distillation provided 93.2 gm of oil. b.p. 141°-143°/0.5 Torr.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04476311 |
| 출처 데이터셋 | uspto-grants-1984_10 |
| ORD ID | ord-312d2c2fdff149489cd828aa97a97e7e |
| 출처 메모 | uspto-grants-1984_10 |