Acetyl chloride → HCID 13390109, 화합물

HRID 1632741

반응식

HRID 1632741 반응식
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([C:11]2[S:15][C:14]([S:16]([NH2:19])(=[O:18])=[O:17])=[CH:13][CH:12]=2)(=[O:10])=[O:9])=[CH:4][CH:3]=1.C(N(CC)CC)C.[C:27](Cl)(=[O:29])[CH3:28]>CC(C)=O>[C:27]([O:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([C:11]2[S:15][C:14]([S:16](=[O:17])(=[O:18])[NH2:19])=[CH:13][CH:12]=2)(=[O:9])=[O:10])=[CH:4][CH:3]=1)(=[O:29])[CH3:28]

참가 물질

5

반응물 3

HCID 6367Acetyl chlorideHCID 8471TriethylamineHCID 127368925-(4-Hydroxyphenyl)sulfonylthiophene-2-sulfonamide

생성물 1

HCID 13390109HCID 13390109, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A solution of 5-[(4-hydroxyphenyl)sulfonyl]thiophene-2-sulfonamide (3.19 g; 0.01 mole) in acetone (60 ml) at -10° was treated with triethylamine (1.11 g; 0.011 mole). Then acetyl chloride (0.86 g; 0.011 mole) was added, dropwise, during 5 minutes at -10°.

출처 및 근거

ORD 기록
ord-6e9e351226344edcaa98445708c6cfa9
출처 데이터셋
uspto-grants-1984_10
특허 번호
US04477466

연결된 노트

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