2-Ethylbutyraldehyde → 3,7-Diethyl-5-azanona-3,5-diene

HRID 1632820노트

반응식

[OH-].[NH4+:2].[CH2:3]([CH:5]([CH2:8][CH3:9])[CH:6]=O)[CH3:4]>>[CH2:3]([C:5](=[CH:6][N:2]=[CH:6][CH:5]([CH2:8][CH3:9])[CH2:3][CH3:4])[CH2:8][CH3:9])[CH3:4]

참가 물질

반응물 2

HCID 73592-Ethylbutyraldehyde

HCID 14923Ammonium Hydroxide

생성물 1

HCID 124134703,7-Diethyl-5-azanona-3,5-diene수율 76.5%

실험 절차

To a sample of 250 grams of 28% ammonium hydroxide was added 215 grams of 2-ethylbutyraldehyde and the heterogeneous mixture was stirred for 18 hours at ambient temperature. The resulting organic layer was separated, and after drying, slowly distilled at atmospheric pressure to yield 148.8 grams of 3,7-diethyl-5-azanona-3,5-diene.

후처리

customThe resulting organic layer was separated
customafter drying
distillationslowly distilled at atmospheric pressure

출처 및 근거

ORD 기록: ord-a939361dc65c4703b98228c5bcdd720d
출처 데이터셋: uspto-grants-1984_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04477674

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