Sodium methanethiolate → HCID 13377373, 화합물

HRID 1632992노트

반응식

HRID 1632992 반응식
Cl[C:2]1[N:7]2[C:8]([CH3:11])=[N:9][CH:10]=[C:6]2[CH:5]=[C:4]([Cl:12])[N:3]=1.[CH3:13][S-:14].[Na+]>>[Cl:12][C:4]1[N:3]=[C:2]([S:14][CH3:13])[N:7]2[C:8]([CH3:11])=[N:9][CH:10]=[C:6]2[CH:5]=1

참가 물질

3

반응물 2

HCID 4378561Sodium methanethiolateHCID 133773425,7-Dichloro-3-methylimidazo[1,5-c]pyrimidine

생성물 1

HCID 13377373HCID 13377373, 화합물

실험 절차

Using the method of Example 53, 5,7-dichloro-3-methylimidazo[1,5-c]pyrimidine (from Example 35) was reacted with sodium methanethiolate to provide yellow solid 7-chloro-3-methyl-5-methylthioimidazo[1,5-c]pyrimidine, m.p. 153°-155° C. Analysis: Calculated for C8H8ClN3S: %C, 45.0; %H, 3.8; %N, 19.7; Found: %C, 44.8; %H, 3.5; %N, 19.7.

출처 및 근거

ORD 기록
ord-7092a73eff3c4b248e1a59675ab96c23
출처 데이터셋
uspto-grants-1984_10
특허 번호
US04478835

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