참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Paroxetine | HCID 43815 | — |
| 반응물 | Potassium Bromide | HCID 253877 | — |
| 반응물 | Tamsulosin Hydrochloride | HCID 5362376 | — |
| 생성물 | Paroxetine Hydrochloride | HCID 62878 | — |
반응 단계
The composition of the solid was tested by FTIR. A Nicolet Magna IR System 750 Fourier Transform Infrared Spectrometer controlled via Nicolet Omnic ESP® software was used to obtain the spectra. A KBr beamsplitter was used and data was collected over 4000−400 cm−1 with a resolution of 4 cm−1. An MCT-A detector, cooled with liquid nitrogen, was used. The sample compartment was under constant nitrogen purge. The aperture was set at 28, the micro velocity was 1.8988 and the gain setting was 1. The contact sampler attachment, which is a horizontal internal reflection accessory, with a trough cell, containing the ZnSe 45° ATR crystal, was used. The background spectrum was air. The spectrum was obtained by averaging 100 scans. The findings were consistent with published spectra for paroxetine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06503927B1 |
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| 출처 데이터셋 | uspto-grants-2003_01 |
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| ORD ID | ord-7122681899ae4fe88d17f372baa3e058 |
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| 출처 메모 | uspto-grants-2003_01 |
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