Phenyl isocyanate → HCID 3297718, 화합물

HRID 1634797노트

반응식

HRID 1634797 반응식
[CH2:1]([NH2:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:10]1([N:16]=[C:17]=[O:18])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>C1COCC1>[CH2:1]([NH:9][C:17]([NH:16][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=[O:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

참가 물질

4

반응물 2

HCID 7672Phenyl isocyanateHCID 8143Octylamine

생성물 1

HCID 3297718HCID 3297718, 화합물수율 98.3%

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

A solution of octyl amine (22.79 g, 176 mmol) and phenyl isocyanate (21 g, 176 mmol) in THF (200 ml) at 0° C. was stirred for 2 hours. The solvent was evaporated in vacuo and the residue was triturated with hexane to give 43 g of final product (173 mmol).

후처리

  1. customThe solvent was evaporated in vacuo
  2. customthe residue was triturated with hexane

출처 및 근거

ORD 기록
ord-60d621653d5746489f7203d49391a857
출처 데이터셋
uspto-grants-2003_01
특허 번호
US06506901B2

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